Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C22H21FNO3P |
| M r | 397.37 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 140 |
| a, b, c () | 18.3667(8), 5.7898(2), 19.7710(7) |
| () | 110.870(4) |
| V (3) | 1964.50(13) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 0.17 |
| Crystal size (mm) | 0.40 0.11 0.07 |
| Data collection | |
| Diffractometer | Oxford Diffraction Xcalibur 3/Sapphire3 CCD |
| Absorption correction | Multi-scan (CrysAlis PRO; Oxford Diffraction, 2010 ▸) |
| T min, T max | 0.790, 1.000 |
| No. of measured, independent and observed [I > 2(I)] reflections | 32284, 4518, 3624 |
| R int | 0.054 |
| (sin /)max (1) | 0.650 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.044, 0.097, 1.05 |
| No. of reflections | 4518 |
| No. of parameters | 253 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.26, 0.34 |