| Crystal data |
| Chemical formula |
C14H25NO3
|
|
M
r
|
255.35 |
| Crystal system, space group |
Monoclinic, P21
|
| Temperature (K) |
150 |
|
a, b, c () |
6.3300(1), 22.0241(5), 10.1179(2) |
| () |
95.2083(12) |
|
V (3) |
1404.74(5) |
|
Z
|
4 |
| Radiation type |
Mo K
|
| (mm1) |
0.08 |
| Crystal size (mm) |
0.44 0.42 0.28 |
| |
| Data collection |
| Diffractometer |
Bruker Kappa APEXII DUO |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2008 ▸) |
|
T
min, T
max
|
0.92, 0.98 |
| No. of measured, independent and observed [I > 2(I)] reflections |
42775, 6792, 6514 |
|
R
int
|
0.027 |
| (sin /)max (1) |
0.660 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.031, 0.082, 1.06 |
| No. of reflections |
6792 |
| No. of parameters |
343 |
| No. of restraints |
1 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
|
max, min (e 3) |
0.24, 0.15 |
| Absolute structure |
Flack x determined using 3097 quotients [(I
+)(I
)]/[(I
+)+(I
)] (Parsons et al., 2013 ▸) |
| Absolute structure parameter |
0.21(19) |
