Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [CrCl3(C15H12N4)] |
| M r | 406.64 |
| Crystal system, space group | Orthorhombic, P n m a |
| Temperature (K) | 150 |
| a, b, c () | 15.152(13), 13.704(12), 8.014(7) |
| V (3) | 1664(2) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 1.17 |
| Crystal size (mm) | 0.06 0.05 0.04 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD area detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2014 ▸) |
| No. of measured, independent and observed [I > 2(I)] reflections | 15895, 1779, 1401 |
| R int | 0.061 |
| (sin /)max (1) | 0.625 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.038, 0.113, 1.20 |
| No. of reflections | 1779 |
| No. of parameters | 118 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.66, 0.51 |