| Crystal data |
| Chemical formula |
[Cr(NCS)2(C2H8N2)2]2[ZnCl4] |
|
M
r
|
783.90 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c () |
7.6870(15), 13.853(3), 14.560(3) |
| , , () |
92.74(3), 92.76(3), 90.21(3) |
|
V (3) |
1546.9(5) |
|
Z
|
2 |
| Radiation type |
Synchrotron, = 0.62998 |
| (mm1) |
1.50 |
| Crystal size (mm) |
0.10 0.03 0.03 |
| |
| Data collection |
| Diffractometer |
ADSC Q210 CCD area detector |
| Absorption correction |
Empirical (using intensity measurements) (HKL3000sm SCALEPACK; Otwinowski Minor, 1997 ▸) |
|
T
min, T
max
|
0.865, 0.956 |
| No. of measured, independent and observed [I > 2(I)] reflections |
17036, 8546, 8434 |
|
R
int
|
0.014 |
| (sin /)max (1) |
0.696 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.018, 0.049, 1.03 |
| No. of reflections |
8546 |
| No. of parameters |
322 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.48, 0.60 |
