Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Re2Cl6(C3H7NO2)2]1.5H2O |
| M r | 790.32 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 223 |
| a, b, c () | 8.2884(9), 17.4526(14), 13.2715(14) |
| () | 107.838(3) |
| V (3) | 1827.5(3) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 14.13 |
| Crystal size (mm) | 0.25 0.22 0.14 |
| Data collection | |
| Diffractometer | Siemens SMART CCD area detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2008 ▸) |
| T min, T max | 0.139, 0.267 |
| No. of measured, independent and observed [I > 2(I)] reflections | 11029, 4413, 4235 |
| R int | 0.027 |
| (sin /)max (1) | 0.665 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.031, 0.075, 1.26 |
| No. of reflections | 4413 |
| No. of parameters | 210 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 1.70, 1.62 |