Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C22H17NO4 |
| M r | 359.37 |
| Crystal system, space group | Triclinic, P
|
| Temperature (K) | 293 |
| a, b, c () | 10.1924(3), 10.8732(3), 16.9675(6) |
| , , () | 97.926(2), 93.711(2), 107.729(2) |
| V (3) | 1762.61(10) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 0.09 |
| Crystal size (mm) | 0.35 0.35 0.30 |
| Data collection | |
| Diffractometer | Bruker Kappa APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2004 ▸) |
| T min, T max | 0.833, 1.000 |
| No. of measured, independent and observed [I > 2(I)] reflections | 39509, 10197, 4932 |
| R int | 0.034 |
| (sin /)max (1) | 0.704 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.062, 0.213, 1.05 |
| No. of reflections | 10197 |
| No. of parameters | 525 |
| No. of restraints | 122 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.38, 0.18 |