| Bruker APEXII CCD area-detector diffractometer | 1356 independent reflections |
| Radiation source: fine-focus sealed tube | 1213 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.034 |
| φ and ω scans | θmax = 25.1°, θmin = 2.6° |
| Absorption correction: multi-scan (SADABS; Bruker, 2007) | h = −9→9 |
| Tmin = 0.148, Tmax = 0.493 | k = −5→4 |
| 6211 measured reflections | l = −25→25 |
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