Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C14H15N5OS |
| M r | 301.37 |
| Crystal system, space group | Monoclinic, P21/n |
| Temperature (K) | 100 |
| a, b, c () | 7.3620(2), 11.9369(4), 16.6755(5) |
| () | 100.191(3) |
| V (3) | 1442.30(8) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 0.23 |
| Crystal size (mm) | 0.40 0.35 0.12 |
| Data collection | |
| Diffractometer | Oxford Diffraction Xcalibur Eos |
| Absorption correction | Multi-scan (CrysAlis PRO; Agilent, 2014 ▸) |
| T min, T max | 0.913, 0.973 |
| No. of measured, independent and observed [I > 2(I)] reflections | 37668, 4359, 3829 |
| R int | 0.033 |
| (sin /)max (1) | 0.724 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.033, 0.083, 1.08 |
| No. of reflections | 4359 |
| No. of parameters | 197 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| max, min (e 3) | 0.49, 0.28 |