| Bruker APEXII CCD diffractometer | 2458 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.024 |
| φ and ω scans | θmax = 72.0°, θmin = 6.3° |
| Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −15→14 |
| Tmin = 0.808, Tmax = 0.879 | k = −16→16 |
| 9639 measured reflections | l = −9→8 |
| 2597 independent reflections |