| Crystal data |
| Chemical formula |
[Tb(C28H28N4O2)(NO3)] |
|
M
r
|
673.47 |
| Crystal system, space group |
Orthorhombic, C2221
|
| Temperature (K) |
100 |
|
a, b, c () |
8.5947(6), 18.2401(17), 16.9272(13) |
|
V (3) |
2653.6(4) |
|
Z
|
4 |
| Radiation type |
Mo K
|
| (mm1) |
2.71 |
| Crystal size (mm) |
0.43 0.20 0.20 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Venture/Photon 100 CMOS |
| Absorption correction |
Multi-scan (SADABS2014/2; Bruker, 2014 ▸) |
|
T
min, T
max
|
0.581, 0.746 |
| No. of measured, independent and observed [I > 2(I)] reflections |
75009, 3320, 3289 |
|
R
int
|
0.020 |
| (sin /)max (1) |
0.668 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.010, 0.027, 1.15 |
| No. of reflections |
3320 |
| No. of parameters |
178 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.87, 0.30 |
| Absolute structure |
Flack x determined using 1431 quotients [(I
+)(I
)]/[(I
+)+(I
)] (Parsons Flack, 2004 ▸) |
| Absolute structure parameter |
0.0107(19) |
