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. 2014 Oct 22;16(21):5656–5659. doi: 10.1021/ol502731p

Table 1. 1H (600 MHz) and 13C (100 MHz) NMR Data of 1 and 2 in CD3OD.

  1
2
no. δH, mult (J, Hz) δC δH, mult (J, Hz) δC
2 7.21, s 125.7, CH 7.19, s 124.6, CH
3   111.9, C   111.1, C
4 7.62, d (8.5) 120.5, CH 7.63, d (7.9) 119.3, CH
5 6.97, dd (8.5, 1.8) 120.2, CH 7.00, t (7.3) 119.7, CH
6   128.2, C 7.08, t (7.3) 122.3, CH
7 7.31, d (1.8) 111.5, CH 7.32, d (8.1) 112.2, CH
8   138.3, C   138.0, C
9   127.6, C   128.8, C
10 3.43, dd (14.8, 4.6) 3.19, dd (14.8, 8.8) 28.3, CH2 3.41, dd (14.8, 5.0) 3.23, dd (14.8, 8.6) 28.4, CH2
11 4.87, dd (8.8, 4.6) 55.0, CH 4.93, dd (8.6, 5.0) 55.1, CH
13   170.3, C   170.3, C
14   127.5, C   127.6, C
15   154.3, C   154.4, C
16 6.66, d (8.8) 115.5, CH 6.66, d (8.8) 115.5, CH
17 7.16, d (8.8) 131.2, CH 7.16, d (8.7) 131.2, CH
18   125.6, C   125.6, C
19   135.2, C   135.2, C
20   175.4, C   175.5, C
21 2.07, s 17.1, CH3 2.06, s 17.0, CH3