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. Author manuscript; available in PMC: 2015 Mar 15.
Published in final edited form as: Bioorg Med Chem. 2014 Feb 6;22(6):1889–1898. doi: 10.1016/j.bmc.2014.01.052

Table 1. 13C NMR data for antiaritoxioside A-G (17) and antiarotoxinin B (8).

Carbon 1 2 3 4 5 6 7 8
1 36.3 26.9 25.3 26.9 26.7 22.0 23.6 25.8
2 22.4 28.7 27.4 28.6 27.9 26.4 26.8 28.6
3 72.9 73.9 73.8 73.8 73.2 72.3 74.1 67.8
4 32.1 35.6 34.8 35.6 35.1 30.0 36.1 36.1
5 72.9 74.7 73.1 74.2 74.3 30.4 73.4 74.5
6 43.3 35.8 35.1 35.9 36.5 33.2 40.8 37.8
7 28.4 24.3 24.5 24.8 24.7 26.0 21.3 24.4
8 42.3 40.7 41.3 40.4 40.4 48.2 41.2 39.0
9 41.0 40.2 39.4 37.5 37.7 42.0 37.3 40.0
10 55.7 74.4 74.4 74.7 74.4 34.0 39.2 41.3
11 23.5 21.6 22.8 30.8 30.7 22.1 26.1 22.0
12 39.9 40.0 40.4 74.7 74.7 39.7 31.4 40.3
13 50.2 50.1 50.3 56.7 56.9 50.1 51.9 47.8
14 84.8 84.6 85.0 85.0 85.1 83.8 86.7 83.8
15 33.4 33.0 33.0 33.4 33.4 32.2 33.7 33.1
16 27.2 27.5 27.2 27.9 29.2 22.1 34.3 19.0
17 51.5 51.3 51.3 46.4 46.2 51.4 87.8 51.5
18 16.3 16.3 16.3 10.3 10.3 16.4 13.1 15.5
19 176.7 17.0 17.4
20 176.1 176.3 176.4 176.7 176.8 176.0 174.0 71.1
21 73.8 73.8 73.8 74.0 74.1 73.6 73.8 65.8
22 117.6 117.7 117.6 117.5 117.4 117.6 116.6
23 174.6 174.8 174.6 174.7 174.8 174.5 173.2
1′ 99.8 100.8 99.3 100.7 99.4 99.8 99.8
2′ 72.7 72.6 72.2 72.6 69.8 72.9 69.6
3′ 72.8 73.0 73.1 72.9 73.6 72.9 73.8
4′ 74.3 73.9 73.8 73.7 73.7 74.1 73.3
5′ 69.9 70.7 70.8 70.7 70.0 70.0 70.0
6′ 18.6 18.6 18.8 18.6 17.0 18.6 17.3

δ Value in pyridine-d5 (100 MHz).

δ Value in pyridine-d5 (75 MHz).