Table 1.
Data collection and refinement statistics
| Ser65-phosphoUb | |
|---|---|
| Data collection | |
| Space group | P1 |
| Cell dimensions | |
| a, b, c (Å) | 49.56, 53.29, 56.87 |
| α, β, γ (°) | 96.86, 104.94, 110.96 |
| Resolution (Å)a | 32.28–1.90 (1.94–1.90) |
| Rmergea | 0.124 (0.425) |
| I/σIa | 4.6 (2.1) |
| Completeness (%)a | 97.3 (96.3) |
| Redundancya | 1.8 (1.8) |
| Refinement | |
| Resolution (Å) | 32.28–1.90 |
| No. reflections/test set | 39,071/1,904 |
| Rwork/Rfree | 0.193/0.238 |
| No. atoms | |
| Protein | 4,579 (587 aa) |
| Ligand/ion | 35 |
| Water | 356 |
| B-factors | |
| Protein | 27.3 |
| Ligand/ion | 45.8 |
| Water | 35.4 |
| R.m.s. deviations | |
| Bond lengths (Å) | 0.007 |
| Bond angles (°) | 1.00 |
a
Values in parentheses are for highest resolution shell.