Table 1. X-ray diffraction and refinement statistics.
Crystal | Pre-TS cleavage Mos1 PEC | |
---|---|---|
PDB ID | 4U7B | |
Space group | C222(1) | |
Cell dimensions | a = 96.2 Å, b = 339.5 Å, c = 160.2 Å | |
Wavelength (Å) | 0.97625 | |
Average mosaicity | 0.46 | |
Overall | Outer shell | |
Resolution (Å) | 92.51–3.09 | 3.27–3.09 |
Rmerge | 0.134 | 0.442 |
Total observations | 385605 | 56422 |
Unique observations | 47937 | 6890 |
< I>/σ<I> | 8.9 | 3.4 |
Completeness (%) | 99.7 | 99.7 |
Multiplicity | 8.0 | 8.2 |
Rwork | 0.229 | |
Rfree | 0.262 | |
r.m.s.d. from ideality | 0.0051 | |
Bond Length (Å) | ||
Bond angle (deg) | 0.982 | |
Chirality (Å) | 0.0675 | |
Ramachandran plot: preferred (%) | 94.31 | |
Allowed (%) | 5.59 | |
Outliers (%) | 0.1 | |
Average B-factor (Å2) | 108.0 | |
Wilson B-factor (Å2) | 79.6 |