Table 3.
Linearity data, limits of quantitation (LOQ) and limits of detection (LOD) in serum and liver samples
Calibration curves of serum samples | Calibration curves of liver samples | |||||||||
BAs | calibration range | correlation coefficient | LOQ (S/N=10) |
LOD (S/N=3) |
BAs | calibration range | correlation coefficient | LOQ (S/N=10) |
LOD (S/N=3) |
|
ng/mL | r2 | ng/mL | ng/mL | ng/g liver |
r2 | ng/g liver |
ng/g liver |
|||
C | 0.25-5000 | 0.999 | 0.25 | < 0.25 | C | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
TC | 0.25-5000 | 0.999 | 0.25 | < 0.25 | TC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
GC | 0.25-5000 | 0.999 | 0.25 | < 0.25 | GC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
CDC | 0.5-5000 | 0.998 | 0.5 | 0.25 | CDC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
TCDC | 0.25-5000 | 0.998 | 0.25 | < 0.25 | TCDC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
GCDC | 0.25-5000 | 0.999 | 0.25 | < 0.25 | GCDC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
UDC | 0.5-5000 | 0.999 | 0.5 | 0.25 | UDC | 7.5-50000 | 0.999 | 7.5 | 5 | |
TUDC | 0.25-5000 | 0.999 | 0.25 | < 0.25 | TUDC | 2.5-50000 | 0.99 | 2.5 | < 2.5 | |
GUDC | 0.5-5000 | 0.999 | 0.5 | 0.25 | GUDC | 2.5-50000 | 0.996 | 2.5 | < 2.5 | |
DC | 0.5-5000 | 0.999 | 0.5 | 0.25 | DC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
TDC | 0.25-5000 | 0.998 | 0.25 | < 0.25 | TDC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
GDC | 0.25-5000 | 0.999 | 0.25 | < 0.25 | GDC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
LC | 0.75-5000 | 0.996 | 0.75 | 0.5 | LC | 7.5-50000 | 0.999 | 7.5 | 5 | |
TLC | 0.25-5000 | 0.996 | 0.25 | < 0.25 | TLC | 2.5-50000 | 0.998 | 2.5 | < 2.5 | |
GLC | 0.25-5000 | 0.999 | 0.25 | < 0.25 | GLC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
DHC | 7.5-5000 | 0.993 | 7.5 | 2.5 | DHC | 25-50000 | 0.99 | 25 | 10 | |
TDHC | 0.5-5000 | 0.999 | 0.5 | 0.25 | TDHC | 2.5-50000 | 0.998 | 2.5 | < 2.5 | |
GDHC | 0.75-5000 | 0.999 | 0.75 | 0.5 | GDHC | 10-50000 | 0.999 | 10 | 5 | |
αMC | 0.5-5000 | 0.999 | 0.5 | 2.5 | αMC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
βMC | 0.5-5000 | 0.999 | 0.5 | 0.25 | βMC | 2.5-50000 | 0.999 | 2.5 | < 2.5 | |
HDC | 0.5-5000 | 0.999 | 0.5 | 0.25 | HDC | 2.5-50000 | 0.996 | 2.5 | < 2.5 |