Table 1. Chemical shifts for ONC201 1H and 13C NMR analysis in d6-DMSO at 25°C Positions are defined in the chemical structure to the right.
Position | 1H | 13C | |
---|---|---|---|
2 | -- | 146.97 | |
4 | 2.56/2.56 | 25.61 | |
5 | 2.65/2.65 | 48.14 | |
6 | -- | 99.11 | |
7 | 3.05/3.05 | 48.41 | |
8 | -- | 151.85 | |
10 | -- | 160.83 | |
11 | 3.96/3.96 | 46.26 | |
12 | 3.68/3.68 | 49.88 | |
14 | 3.63/3.63 | 61.05 | |
15 | -- | 138.04 | |
16 | 4.87/4.87 | 41.98 | |
17 | -- | 134.74 | |
19 | 7.33 | 128.54 | |
20 | 7.33 | 129.00 | |
21 | 7.26 | 127.41 | |
22 | 7.33 | 129.00 | |
23 | 7.33 | 128.54 | |
24 | 6.89 | 125.07 | |
25 | 7.10 | 126.46 | |
26 | 7.09 | 126.14 | |
27 | 7.13 | 129.46 | |
28 | -- | 134.74 | |
29 | 2.31 | 18.38 |