| Crystal data |
| Chemical formula |
[ZnCl2(C15H12N2)2] |
|
M
r
|
576.80 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c () |
9.2410(6), 9.2595(5), 16.4106(10) |
| , , () |
87.770(1), 88.819(1), 72.823(1) |
|
V (3) |
1340.50(14) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
1.14 |
| Crystal size (mm) |
0.40 0.30 0.30 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD area detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2008 ▸) |
|
T
min, T
max
|
0.658, 0.726 |
| No. of measured, independent and observed [I > 2(I)] reflections |
8564, 5308, 4067 |
|
R
int
|
0.025 |
| (sin /)max (1) |
0.619 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.037, 0.091, 1.00 |
| No. of reflections |
5308 |
| No. of parameters |
334 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.31, 0.35 |
