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. 2015 Feb 18;71(Pt 3):275–277. doi: 10.1107/S2056989015001747
Bruker D8 Vantage single-crystal CCD diffractometer 7739 independent reflections
Radiation source: fine-focus sealed tube 5760 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.089
Detector resolution: 8.3 pixels mm-1 θmax = 25.1°, θmin = 2.3°
Sets of exposures each taken over 0.5° ω rotation scans h = −9→9
Absorption correction: multi-scan (SADABS; Bruker, 2013) k = −22→22
Tmin = 0.852, Tmax = 1.000 l = −35→35
44800 measured reflections