Table 2. Experimental details.
| Crystal data | |
| Chemical formula | [Rh(C10H15)Cl(C13H12ClN3)]Cl |
| M r | 554.74 |
| Crystal system, space group | Orthorhombic, P b c a |
| Temperature (K) | 173 |
| a, b, c () | 13.0774(5), 13.4537(5), 26.5153(9) |
| V (3) | 4665.1(3) |
| Z | 8 |
| Radiation type | Mo K |
| (mm1) | 1.09 |
| Crystal size (mm) | 0.21 0.20 0.13 |
| Data collection | |
| Diffractometer | STOE IPDS diffractometer |
| Absorption correction | Empirical (using intensity measurements) (DIFABS; Walker Stuart, 1983 ▸) |
| T min, T max | 0.629, 0.890 |
| No. of measured, independent and observed [I > 2(I)] reflections | 82717, 6320, 4619 |
| R int | 0.074 |
| (sin /)max (1) | 0.687 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.032, 0.054, 0.96 |
| No. of reflections | 6320 |
| No. of parameters | 281 |
| H-atom treatment | H atoms treated by a mixture of independent and constrained refinement |
| max, min (e 3) | 0.48, 0.62 |