Table 2. Compound specific liquid chromatography/ mass spectrometry parameters for flurbiprofen (FLB), 4’-hydroxyflurbiprofen (OHF) and the respective deuterated internal standards FLB-d3 and OHF-d3.
Compound | Transition | DP (V) | CE (V) | Retention time (min) |
---|---|---|---|---|
FLB | 243 → 199 | -26 | -10 | 8.1 |
OHF | 259 → 215 | -16 | -12 | 7.7 |
FLB-d3 | 246 → 202 | -21 | -12 | 8.1 |
OHF-d3 | 262 → 218 | -21 | -12 | 7.7 |
DP, declustering potential; CE, collision energy.