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. 2015 Feb 27;11:294–301. doi: 10.3762/bjoc.11.34

Table 3.

Electrochemical synthesis of 12a using different additives.

graphic file with name Beilstein_J_Org_Chem-11-294-i004.jpg

Entrya additive yieldb [%] c.e.c [%] drd [12a:12b]

1 9 63 25 6.8
2 10 42 17 5.6
3 11 78 31 8.6
4 Inline graphic
13
73 29 4.4

aAnode: platinum; byield determined by GC (internal standard); cc.e. = current efficiency; dratio determined by NMR spectroscopy.