Table 3.
Electrochemical synthesis of 12a using different additives.
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Entrya | additive | yieldb [%] | c.e.c [%] | drd [12a:12b] |
1 | 9 | 63 | 25 | 6.8 |
2 | 10 | 42 | 17 | 5.6 |
3 | 11 | 78 | 31 | 8.6 |
4 |
![]() 13 |
73 | 29 | 4.4 |
aAnode: platinum; byield determined by GC (internal standard); cc.e. = current efficiency; dratio determined by NMR spectroscopy.