Skip to main content
. 2015 Feb 13;11:242–248. doi: 10.3762/bjoc.11.27

Table 1.

Reaction of 3a-X (X = Br, I) with different bases.a

graphic file with name Beilstein_J_Org_Chem-11-242-i001.jpg

% Yield of productb
X = Br X = I


Base 4a-Br 5a-Br 6a 4a-Ir 5a-I 6a

Et3N/CH2Cl2 83 ND ND 85 ND 1
NaOH/H2O ND 89 2 ND 84 1
NaOMe/MeOH ND ND 95 ND ND 96

aThe electrolysis was carried out using 1.3 equiv of Bu4NBr or Bu4NI (based on the alkene which was added after electrolysis) with 2.1 F/mol of electricity based on Bu4NBr or Bu4NI. bYields were determined by GC.