| Crystal data |
| Chemical formula |
C17H18N2O2S2
|
|
M
r
|
346.45 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c () |
9.6432(5), 10.796(1), 16.1673(10) |
| , , () |
90.899(6), 97.203(5), 91.200(6) |
|
V (3) |
1669.2(2) |
|
Z
|
4 |
| Radiation type |
Cu K
|
| (mm1) |
2.98 |
| Crystal size (mm) |
0.15 0.06 0.04 |
| |
| Data collection |
| Diffractometer |
Oxford Diffraction Gemini |
| Absorption correction |
Multi-scan (CrysAlis RED; Oxford Diffraction, 2002 ▸) |
|
T
min, T
max
|
0.74, 0.89 |
| No. of measured, independent and observed [I > 2(I)] reflections |
23678, 6592, 5514 |
|
R
int
|
0.028 |
| (sin /)max (1) |
0.622 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.037, 0.106, 0.99 |
| No. of reflections |
6567 |
| No. of parameters |
415 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.44, 0.33 |
