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. 2015 Jan 31;71(Pt 2):234–237. doi: 10.1107/S2056989015001632

Table 2. Experimental details.

Crystal data
Chemical formula MnSn(OH)6
M r 275.68
Crystal system, space group Tetragonal, P42/n
Temperature (K) 293
a, c () 7.8655(4), 7.7938(6)
V (3) 482.17(5)
Z 4
Radiation type Mo K
(mm1) 7.74
Crystal size (mm) 0.05 0.05 0.04
 
Data collection
Diffractometer Bruker APEXII CCD area detector
Absorption correction Multi-scan (SADABS; Bruker, 2004)
T min, T max 0.698, 0.747
No. of measured, independent and observed [I > 2(I)] reflections 4394, 1272, 681
R int 0.020
(sin /)max (1) 0.863
 
Refinement
R[F 2 > 2(F 2)], wR(F 2), S 0.021, 0.056, 1.00
No. of reflections 1272
No. of parameters 56
H-atom treatment All H-atom parameters refined
max, min (e 3) 0.55, 0.54

Computer programs: APEX2 and SAINT (Bruker, 2004), SHELXS97 and SHELXL97 (Sheldrick, 2008), XtalDraw (Downs Hall-Wallace, 2003) and publCIF (Westrip, 2010).