| Crystal data |
| Chemical formula |
[Cu(C6H4NO2)2(C16H38N6)] |
|
M
r
|
622.27 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c () |
8.0490(16), 8.3000(17), 11.175(2) |
| , , () |
81.16(3), 87.14(3), 86.68(3) |
|
V (3) |
735.8(3) |
|
Z
|
1 |
| Radiation type |
Synchrotron, = 0.630 |
| (mm1) |
0.57 |
| Crystal size (mm) |
0.08 0.03 0.03 |
| |
| Data collection |
| Diffractometer |
ADSC Q210 CCD area detector |
| Absorption correction |
Empirical (using intensity measurements) (HKL3000sm SCALEPACK; Otwinowski Minor, 1997 ▸) |
|
T
min, T
max
|
0.958, 0.983 |
| No. of measured, independent and observed [I > 2(I)] reflections |
7574, 3882, 3608 |
|
R
int
|
0.018 |
| (sin /)max (1) |
0.696 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.030, 0.086, 1.09 |
| No. of reflections |
3882 |
| No. of parameters |
188 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.43, 0.62 |
