| Crystal data |
| Chemical formula |
[Cu(ClO4)2(C16H38N6)] |
|
M
r
|
576.96 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c () |
8.2230(16), 8.3600(17), 10.039(2) |
| , , () |
92.87(3), 96.12(3), 116.60(3) |
|
V (3) |
609.8(3) |
|
Z
|
1 |
| Radiation type |
Synchrotron, = 0.62998 |
| (mm1) |
0.84 |
| Crystal size (mm) |
0.10 0.10 0.03 |
| |
| Data collection |
| Diffractometer |
ADSC Q210 CCD area detector |
| Absorption correction |
Empirical (using intensity measurements) HKL3000sm
SCALEPACK (Otwinowski Minor, 1997 ▸) |
|
T
min, T
max
|
0.921, 0.975 |
| No. of measured, independent and observed [I > 2(I)] reflections |
6292, 3195, 2536 |
|
R
int
|
0.025 |
| (sin /)max (1) |
0.696 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.034, 0.091, 1.02 |
| No. of reflections |
3195 |
| No. of parameters |
152 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.29, 0.86 |
