Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C13H10O2 |
| M r | 198.21 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 130 |
| a, b, c () | 9.5296(7), 10.1383(7), 11.1595(7) |
| () | 103.922(6) |
| V (3) | 1046.49(13) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 0.08 |
| Crystal size (mm) | 0.50 0.45 0.32 |
| Data collection | |
| Diffractometer | Agilent Xcalibur Atlas Gemini |
| Absorption correction | Multi-scan (CrysAlis PRO; Agilent, 2011 ▸) |
| T min, T max | 0.781, 1 |
| No. of measured, independent and observed [I > 2(I)] reflections | 8114, 2553, 1755 |
| R int | 0.019 |
| (sin /)max (1) | 0.691 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.045, 0.115, 1.04 |
| No. of reflections | 2553 |
| No. of parameters | 136 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.11, 0.17 |