| Rigaku R-AXIS RAPID diffractometer | 1232 reflections with F2 > 2σ(F2) |
| Detector resolution: 10.000 pixels mm-1 | Rint = 0.075 |
| ω scans | θmax = 68.2° |
| Absorption correction: multi-scan (ABSCOR; Higashi, 1995) | h = −6→6 |
| Tmin = 0.687, Tmax = 0.879 | k = −15→15 |
| 12963 measured reflections | l = −14→14 |
| 1350 independent reflections |
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