| Oxford Gemini CCD diffractometer | 7318 independent reflections |
| Radiation source: fine-focus sealed tube | 6793 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.042 |
| ω scans | θmax = 66.0°, θmin = 3.3° |
| Absorption correction: multi-scan (CrysAlis RED; Oxford Diffraction, 2006) | h = −9→9 |
| Tmin = 0.427, Tmax = 1.000 | k = −16→16 |
| 18279 measured reflections | l = −22→23 |