| Bruker SMART 1K CCD area-detector diffractometer | 4850 reflections with I > 2σ(I) |
| Radiation source: fine-focus sealed tube | Rint = 0.032 |
| Graphite monochromator | θmax = 25.0°, θmin = 2.6° |
| ω scan | h = −6→6 |
| 19586 measured reflections | k = −9→9 |
| 6013 independent reflections | l = −22→23 |
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