| Refinement on F2 | Hydrogen site location: mixed |
| Least-squares matrix: full | H atoms treated by a mixture of independent and constrained refinement |
| R[F2 > 2σ(F2)] = 0.030 | w = 1/[σ2(Fo2) + (0.0483P)2 + 0.551P] where P = (Fo2 + 2Fc2)/3 |
| wR(F2) = 0.082 | (Δ/σ)max = 0.002 |
| S = 1.06 | Δρmax = 0.53 e Å−3 |
| 11408 reflections | Δρmin = −0.31 e Å−3 |
| 213 parameters | Absolute structure: Flack (1983), 5353 Friedel pairs |
| 0 restraints | Absolute structure parameter: 0.50 (3) |