| Agilent Xcalibur (Eos, Gemini) diffractometer | 3859 independent reflections |
| Radiation source: Enhance (Cu) X-ray Source | 3209 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.022 |
| Detector resolution: 16.0416 pixels mm-1 | θmax = 71.3°, θmin = 3.1° |
| ω scans | h = −8→8 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2014) | k = −13→11 |
| Tmin = 0.928, Tmax = 1.000 | l = −15→18 |
| 6591 measured reflections |
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