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. 2015 Jan 31;71(Pt 2):231–233. doi: 10.1107/S2056989015000365
Bruker Kappa APEXII CCD diffractometer 1653 independent reflections
Radiation source: fine-focus sealed tube 1557 reflections with I > 2σ(I)
Graphite monochromator Rint = 0.024
ω and φ scans θmax = 25.0°, θmin = 2.4°
Absorption correction: multi-scan (SADABS; Bruker, 2004) h = −33→33
Tmin = 0.887, Tmax = 0.917 k = −10→10
15358 measured reflections l = −8→8