Bruker Kappa APEXII CCD diffractometer | 1653 independent reflections |
Radiation source: fine-focus sealed tube | 1557 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.024 |
ω and φ scans | θmax = 25.0°, θmin = 2.4° |
Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −33→33 |
Tmin = 0.887, Tmax = 0.917 | k = −10→10 |
15358 measured reflections | l = −8→8 |