Table 2.
Src-like module of mouse Btk (217-659) | ||||
---|---|---|---|---|
Data collection | ||||
KAu(CN)2 | DMA | Au2(NO3)3 | native | |
Wavelength (Å) | 0.9474 | 0.9474 | 0.9474 | 0.9474 |
Space group | P31 2 1 | P31 2 1 | P31 2 1 | P31 2 1 |
a,b,c (Å) | 132.2, 132.2, 107.6 | 132.5, 132.5, 107.3 | 131.9, 131.9, 107.6 | 131.8, 131.8, 107.0 |
α,β,γ (°) | 90.0, 90.0, 120.0 | 90.0, 90.0, 120.0 | 90.0, 90.0, 120.0 | 90.0, 90.0, 120.0 |
Resolution (Å) | 43.2–2.6 | 41.7–3.5 | 41.7–3.4 | 40–4.0 |
Rsym (%) | 8.7(>100) | 8.7 (32.7) | 7.5 (32.5) | 5.1 (71.7) |
I/σ(I) | 10.6 (1.1) | 9.7 (3.0) | 12.1 (3.6) | 18.4 (12.3) |
Completeness (%) | 91.9 (69.6) | 92.4 (94.2) | 94.5 (95.9) | 92.3 (100) |
Redundancy | 4.8 (3.5) | 4.3 | 4.1 | N/A |
Wilson B factor | 72.8 | 58.8 | 70.8 | 67.3 |