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. 2014 Feb 24;97(4):1065–1073. doi: 10.1111/jace.12861

Table II.

Phase Composition of the Reactants and Set Cements. The Measured Composition was Determined by Rietveld Refinement of the XRD patterns

Initial powders
Set cements
Nominal composition
Measured composition (XRD/Rietveld refinement)*
Measured composition (XRD/Rietveld refinement)*
Material % α-TCP % β-TCP % α-TCP % β-TCP % HA % α-TCP % β-TCP % CDHA
0% β 100 0 94.9 2.9 2.2 0 3.7 96.3
20% β 80 20 76.7 22.8 0.5 0 21.4 78.6
40% β 60 40 54.8 44.6 0.6 1.5 37.4 61.1
80% β 20 80 17.4 82.1 0.5 0 77.8 22.2
100% β 0 100 2.4 97.5 0.1 0 99.5 0.5
*

Error ± 1%.