Table 1. Data-collection, processing and refinement statistics for TesB.
Values in parentheses are for the highest resolution shell.
| YpTesB (PDB entry 4qfw) | YpTesB + CoA (PDB entry 4r4u) | |
|---|---|---|
| Wavelength () | 0.9537 | 0.9537 |
| Resolution range () | 36.892.00 (2.042.00) | 45.912.20 (2.262.20) |
| Space group | P1211 | P1211 |
| Unit-cell parameters (, ) | a = 51.23, b = 171.62, c = 73.70, = 90, = 109.62, = 90 | a = 550.98, b = 171.37, c = 73.66, = 90, = 109.51, = 90 |
| Total observations | 446767 (25650) | 461970 (33455) |
| Unique reflections | 75550 (4191) | 60243 (4431) |
| Multiplicity | 5.9 (6.1) | 7.7 (7.6) |
| Completeness (%) | 93.9 (87.3) | 100 (100) |
| R merge | 0.103 (0.211) | 0.105 (0.491) |
| R p.i.m. | 0.047 (0.09) | 0.043 (0.206) |
| Mean I/(I) | 10.3 (5.6) | 10.3 (4.1) |
| Wilson B value (2) | 28.85 | 32.44 |
| R cryst | 0.22 | 0.20 |
| R free | 0.27 | 0.26 |
| No. of atoms | ||
| Total | 8667 | 9126 |
| Macromolecules | 8460 | 8712 |
| Water | 207 | 414 |
| R.m.s.d., bonds () | 0.017 | 0.009 |
| R.m.s.d., angles () | 1.613 | 1.152 |
| Ramachandran plot (%) | ||
| Favoured region | 91.8 | 90.4 |
| Allowed region | 7.5 | 9.4 |
| Generously allowed region | 0.7 | 0.2 |
| Disallowed region | 0.0 | 0.0 |