Scheme 1.
Synthesis of UKP13-C6-LKS01 (probe 1). (a) 1) TFA, dichloromethane, 1 hr; 2) DSS (Disuccinimidyl suberate), DIPEA (N,N-diisopropylethylamine), THF, overnight; (b) H2, Pd/C, MeOH/EtOAc, 4 hr; (c) DIPEA, THF, overnight.
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