| Bruker D8 Venture diffractometer | 4395 independent reflections |
| Radiation source: fine-focus sealed tube | 3050 reflections with I > 2σ(I) |
| Multilayered confocal mirror monochromator | Rint = 0.063 |
| Detector resolution: 8.333 pixels mm-1 | θmax = 25.0°, θmin = 2.4° |
| φ and ω scans | h = −15→14 |
| Absorption correction: multi-scan (SADABS; Bruker, 2014) | k = −15→15 |
| Tmin = 0.92, Tmax = 0.99 | l = −16→18 |
| 22512 measured reflections |
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