Bruker D8 Venture diffractometer | 9735 independent reflections |
Radiation source: fine-focus sealed tube | 7339 reflections with I > 2σ(I) |
Multilayered confocal mirror monochromator | Rint = 0.041 |
Detector resolution: 8.333 pixels mm-1 | θmax = 25.0°, θmin = 2.2° |
φ and ω scans | h = −13→13 |
Absorption correction: multi-scan (SADABS; Bruker, 2014) | k = −18→18 |
Tmin = 0.97, Tmax = 0.98 | l = −19→19 |
50997 measured reflections |