Bruker D8 Venture diffractometer | 4480 independent reflections |
Radiation source: fine-focus sealed tube | 3212 reflections with I > 2σ(I) |
Multilayered confocal mirror monochromator | Rint = 0.058 |
Detector resolution: 8.333 pixels mm-1 | θmax = 25.0°, θmin = 2.5° |
φ and ω scans | h = −11→11 |
Absorption correction: multi-scan (SADABS; Bruker, 2014) | k = −23→21 |
Tmin = 0.98, Tmax = 0.99 | l = −16→16 |
23252 measured reflections |