| Agilent Xcalibur Sapphire3 diffractometer | 5881 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 4239 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.075 |
| Detector resolution: 16.0560 pixels mm-1 | θmax = 27.0°, θmin = 2.4° |
| ω scans | h = −8→8 |
| Absorption correction: multi-scan (CrysAlis PRO; Oxford Diffraction, 2013) | k = −11→11 |
| Tmin = 0.981, Tmax = 1.000 | l = −29→29 |
| 34730 measured reflections |
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