Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C26H26N20.5C8H10 |
| M r | 419.57 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 173 |
| a, b, c () | 8.7618(7), 29.450(2), 9.6569(8) |
| () | 114.732(1) |
| V (3) | 2263.2(3) |
| Z | 4 |
| Radiation type | Mo K |
| (mm1) | 0.07 |
| Crystal size (mm) | 0.35 0.21 0.13 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Sheldrick, 1996 ▸) |
| T min, T max | 0.700, 0.746 |
| No. of measured, independent and observed [I > 2(I)] reflections | 25883, 5184, 4102 |
| R int | 0.032 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.048, 0.126, 1.06 |
| No. of reflections | 5184 |
| No. of parameters | 294 |
| No. of restraints | 321 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 0.51, 0.37 |