| Crystal data |
| Chemical formula |
C2H8N+C2HO4
0.5C2H2O4
|
|
M
r
|
180.14 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
100 |
|
a, b, c () |
5.6519(3), 7.5809(4), 10.3100(6) |
| , , () |
75.467(2), 88.120(2), 69.487(2) |
|
V (3) |
399.76(4) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.14 |
| Crystal size (mm) |
0.5 0.3 0.1 |
| |
| Data collection |
| Diffractometer |
Bruker D8 Venture triumph Mo |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2014 ▸) |
|
T
min, T
max
|
0.693, 0.746 |
| No. of measured, independent and observed [I 2(I)] reflections |
10413, 1840, 1655 |
|
R
int
|
0.023 |
| (sin /)max (1) |
0.651 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.028, 0.075, 1.07 |
| No. of reflections |
1840 |
| No. of parameters |
113 |
| H-atom treatment |
H-atom parameters not refined |
|
max, min (e 3) |
0.38, 0.26 |
