Bruker APEXII CCD diffractometer | 1323 independent reflections |
Radiation source: fine-focus sealed tube | 1122 reflections with I > 2σ(I) |
Detector resolution: 8.3333 pixels mm-1 | Rint = 0.026 |
φ and ω scans | θmax = 28.0°, θmin = 3.1° |
Absorption correction: multi-scan (SADABS; Bruker, 2014) | h = −8→8 |
Tmin = 0.81, Tmax = 0.97 | k = −8→8 |
7544 measured reflections | l = −9→9 |