| Rigaku Mercury375R (2x2 bin mode) diffractometer | 2058 independent reflections |
| Radiation source: fine-focus sealed tube | 1769 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.033 |
| Detector resolution: 13.6612 pixels mm-1 | θmax = 25.5°, θmin = 3.1° |
| profile data from ω–scan | h = −12→12 |
| Absorption correction: multi-scan (REQAB; Rigaku, 1998) | k = −12→12 |
| Tmin = 0.797, Tmax = 0.970 | l = −12→12 |
| 9498 measured reflections |
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