| Crystal data |
| Chemical formula |
[Li(C24H34O4P)(CH4O)3]CH4O |
|
M
r
|
552.59 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
123 |
|
a, b, c () |
11.1853(6), 11.5046(6), 14.5237(7) |
| , , () |
90.855(2), 102.859(2), 118.683(1) |
|
V (3) |
1582.21(14) |
|
Z
|
2 |
| Radiation type |
Mo K
|
| (mm1) |
0.13 |
| Crystal size (mm) |
0.60 0.20 0.10 |
| |
| Data collection |
| Diffractometer |
Bruker APEXII CCD area-detector |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2003 ▸) |
|
T
min, T
max
|
0.872, 0.986 |
| No. of measured, independent and observed [I > 2(I)] reflections |
22920, 10353, 8544 |
|
R
int
|
0.021 |
| (sin /)max (1) |
0.732 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.040, 0.112, 1.02 |
| No. of reflections |
10353 |
| No. of parameters |
382 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
|
max, min (e 3) |
0.77, 0.53 |
