| Crystal data |
| Chemical formula |
[Cr(NCS)2(C10H24N4)]2[ZnCl4] |
|
M
r
|
944.15 |
| Crystal system, space group |
Monoclinic, P2/c
|
| Temperature (K) |
260 |
|
a, b, c () |
7.9990(16), 16.532(3), 15.430(3) |
| () |
101.36(3) |
|
V (3) |
2000.5(7) |
|
Z
|
2 |
| Radiation type |
Synchrotron, = 0.610 |
| (mm1) |
1.07 |
| Crystal size (mm) |
0.22 0.19 0.12 |
| |
| Data collection |
| Diffractometer |
ADSC Q210 CCD area detector diffractometer |
| Absorption correction |
Empirical (using intensity measurements) (HKL3000sm
SCALEPACK; Otwinowski Minor, 1997 ▸) |
|
T
min, T
max
|
0.801, 0.883 |
| No. of measured, independent and observed [I > 2(I)] reflections |
20982, 5738, 5500 |
|
R
int
|
0.018 |
| (sin /)max (1) |
0.706 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.025, 0.072, 1.06 |
| No. of reflections |
5738 |
| No. of parameters |
217 |
| H-atom treatment |
H-atom parameters constrained |
|
max, min (e 3) |
0.60, 0.58 |
