| Crystal data |
| Chemical formula |
[Co(C8H4NO2)2(C6H6N2O)2(H2O)2] |
|
M
r
|
631.46 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
296 |
|
a, b, c () |
7.6474(3), 9.9266(4), 10.2782(4) |
| , , () |
78.680(2), 84.200(3), 71.556(2) |
|
V (3) |
725.13(5) |
|
Z
|
1 |
| Radiation type |
Mo K
|
| (mm1) |
0.65 |
| Crystal size (mm) |
0.43 0.29 0.16 |
| |
| Data collection |
| Diffractometer |
Bruker SMART BREEZE CCD |
| Absorption correction |
Multi-scan (SADABS; Bruker, 2012 ▸) |
|
T
min, T
max
|
0.797, 0.901 |
| No. of measured, independent and observed [I > 2(I)] reflections |
16533, 3639, 3419 |
|
R
int
|
0.036 |
| (sin /)max (1) |
0.672 |
| |
| Refinement |
|
R[F
2 > 2(F
2)], wR(F
2), S
|
0.044, 0.119, 1.07 |
| No. of reflections |
3639 |
| No. of parameters |
212 |
| H-atom treatment |
H atoms treated by a mixture of independent and constrained refinement |
|
max, min (e 3) |
0.94, 0.49 |
