Table 3. Experimental details.
| Crystal data | |
| Chemical formula | [Ba(C5HN2O6)(C2O4)0.5(H2O)2] |
| M r | 804.92 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c () | 10.3283(11), 7.9868(8), 13.0760(14) |
| () | 96.419(2) |
| V (3) | 1071.88(19) |
| Z | 2 |
| Radiation type | Mo K |
| (mm1) | 3.76 |
| Crystal size (mm) | 0.16 0.12 0.03 |
| Data collection | |
| Diffractometer | Bruker APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2004 ▸) |
| T min, T max | 0.586, 0.746 |
| No. of measured, independent and observed [I > 2(I)] reflections | 11240, 3410, 2692 |
| R int | 0.036 |
| (sin /)max (1) | 0.736 |
| Refinement | |
| R[F 2 > 2(F 2)], wR(F 2), S | 0.038, 0.093, 1.05 |
| No. of reflections | 3410 |
| No. of parameters | 172 |
| No. of restraints | 6 |
| H-atom treatment | H-atom parameters constrained |
| max, min (e 3) | 2.31, 1.67 |