Skip to main content
. 2015 Apr 22;71(Pt 5):544–546. doi: 10.1107/S2056989015007525

Table 2. Experimental details.

Crystal data
Chemical formula [Ag(C27H36N2)2]ClC4H8O
M r 992.58
Crystal system, space group Monoclinic, P21/n
Temperature (K) 173
a, b, c () 11.9302(3), 18.3390(5), 26.0144(6)
() 103.068(2)
V (3) 5544.2(2)
Z 4
Radiation type Mo K
(mm1) 0.45
Crystal size (mm) 0.31 0.27 0.26
 
Data collection
Diffractometer Stoe IPDS 2
Absorption correction Multi-scan (X-AREA; Stoe Cie, 2001)
T min, T max 0.571, 1.000
No. of measured, independent and observed [I > 2(I)] reflections 111561, 15949, 13800
R int 0.075
(sin /)max (1) 0.705
 
Refinement
R[F 2 > 2(F 2)], wR(F 2), S 0.048, 0.121, 1.05
No. of reflections 15949
No. of parameters 651
No. of restraints 75
H-atom treatment H-atom parameters constrained
max, min (e 3) 1.03, 1.37

Computer programs: X-AREA and X-RED32 (Stoe Cie, 2001), SHELXS97 and XP (Sheldrick, 2008), SHELXL2014 (Sheldrick, 2015), PLATON (Spek, 2009) and publCIF (Westrip, 2010).